Astrochemistry Laboratory
Equipment - Hot Environments Lab - Sciences and Exploration Directorate - NASA's Goddard Space Flight Centerr

Hot Environments Lab - Equipment

Hot Environments Lab - Equipment

Thermogravimetric Analysis (TGA) Systems

Thermogravimetric analysis (TGA) is an analytical technique that determines a material's thermal stability by measuring the weight change as a sample is heated. Our lab has two TGA systems capable of reaching high temperatures.

CAHN TGA

Metal cyclindrical machinery surround in a wire mesh with tubes/pipes coming out of it.
  • Mass balance with mg precision
  • Reaches temperatures up to 1700°C
  • Molybdenum heating elements
  • Capable of reaching high-vacuum
  • Requires solid (powdered or granular) samples

The CAHN TGA system measures the mass-loss rates of a sample, gathering data every 0.5 seconds.

Themys TGA

Bright red cyclindrical machine.
  • Reaches temps up to 2400°C
  • Operates in low-vacuum, or inert carrier gas
  • Alumina and graphite oven wall options
  • Requires solid (powdered or granular) samples

This TGA is capable of high temperature runs with the graphite oven wall insert option and can heat at a max rate of 100°C/min. The mass balance has a high sensitivity with 0.00059µg resolution and can hold up to a 35g sample. This modular system can perform evolved gas analysis of samples with a high temperature coupled FTIR and/or mass spectrometer. An additional coupling enables differential thermal analysis (DTA) for the determination of characteristic temperatures such as mineral melting points or dehydration reactions, and differential scanning calorimetry (DSC) to yield precise determinations of thermodynamic values such as the heat of fusion or heat of crystallization for key species.


FTIR Systems and Cells

Two highly adaptable FTIRs that span the UV through MIR spectral range. Capable of using internal and external beam sources with different beam path options available and multiple detectors. Coupled with modular high temperatures FTIR cells capable of taking spectra of materials at various phases over large temperature and pressure ranges.

Aabspec Cell

Black metal box with a few flexible tubes coming out of it.
  • Temperature: -170°C to 950°C
  • Pressure: vacuum to 138 bar
  • Gases: CO2, N2, SO2, CO, and more
  • Ideal for mid-IR
  • Ideal for solids and gases

Specac Cell

Black and silver metal machinery
  • Temperature: Ambient to 800°C
  • Pressure: vacuum to 69 bar
  • Gases: CO2, N2, SO2, CO, and more
  • Ideal for UV, NIR-FIR
  • Designed for solid, gases, and liquids
  • Transmission, decomposition or specular reflectance modes

Venus Chambers

We have two chambers capable of simulating the temperature, pressure, and chemistry of the Venus environment from the top of the atmosphere down to the surface. These chambers are useful for instrumentation and science investigations.

Black rolling cart with a metal cyclindrical machine in the middle with various tubes, wires, pressure gauges, etc. hanging off of it.
  • 5 in diam x 11 in depth
  • 316 Stainless steel
  • Pressure: vacuum to 96 bar
  • Temperature: ambient to 470°C
  • Gas species: CO2, N2, SO2
  • Feedthroughs; larger - ideal for instruments
  • LabVIEW software records simultaneous temperature and pressure readings
Metal machinery
  • 300 mL
  • Alloy 600 (Inconel)
  • Temperature: ambient to 490°C
  • Pressure: vacuum to 105 bar
  • Gases: CO2, N2, SO2 CO, and more
  • Optional optical window, smaller - quick turnaround time